4-硝基苯-β-D-吡喃海藻糖苷合成路线 (共 8 条)
反应条件
sodium methylate in methanol T=4°C;
参考文献
Carbohydrate research, , vol. 112, # 2 p. 213 - 220
反应条件
1: 18 percent / dimethylformamide / Ambient temperature 2: 83.5 percent / 0.5 M sodium methoxide / methanol / 4 °C View Scheme
参考文献
Carbohydrate research, , vol. 112, # 2 p. 213 - 220
反应条件
1: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C 2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; dichloromethane / 20 °C 3: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: pyridine / 20 °C 2: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C 3: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; dichloromethane / 20 °C 4: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: 18 percent / dimethylformamide / Ambient temperature 2: 83.5 percent / 0.5 M sodium methoxide / methanol / 4 °C View Scheme
参考文献
Carbohydrate research, , vol. 112, # 2 p. 213 - 220
反应条件
acetate buffer T=37°C; pH=4.6; 0.5 h; Enzyme kinetics; Further Variations:Reagents;
参考文献
Gantulga, Dashzeveg; Turan, Yusuf; Bevan, David R.; Esen, Asim
Phytochemistry, 2008 , vol. 69, # 8 p. 1661 - 1670
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in water T=45°C; pH=8.8; 24 h; Enzymatic reaction;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
recombinant α-L-rhamnosidase from Streptomyces avermitilis NBRC14893; bovine serum albumin in aq. buffer T=30°C; pH=6; 0.5 h; Enzymatic reaction; Kinetics;
参考文献
Ichinose, Hitomi; Fujimoto, Zui; Kaneko, Satoshi
Bioscience, Biotechnology and Biochemistry, 2013 , vol. 77, # 1 p. 213 - 216