in neat (no solvent)
allowed to stand in the dark for 16 h at ambient temp. in the presence of a trace of Et2O;
参考文献
Anema, Skelte G.; Audett (nee Christie), Judy A.; Mackay, Kenneth M.; Nicholson, Brian K.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2629 - 2634
in neat (no solvent)
allowed to stand in the dark for 64 h at ambient temp.; identified spectroscopically;
参考文献
Anema, Skelte G.; Audett (nee Christie), Judy A.; Mackay, Kenneth M.; Nicholson, Brian K.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2629 - 2634