5-亚苄基-2,2-二甲基-1,3-二恶烷-4,6-二酮合成路线 （共 31 条）
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
1: α-benzyl Meldrum's acid With potassium hydride in acetonitrile
T=20°C; 0.333333 h; Inert atmosphereGlovebox;
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium in acetonitrile
T=24.84°C; Inert atmosphereGlovebox; Thermodynamic data;
参考文献
Cao, Ying; Zhang, Song-Chen; Zhang, Min; Shen, Guang-Bin; Zhu, Xiao-Qing
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7154 - 7168
反应条件
sodium hydride in N,N-dimethyl-formamide
Corey-Chaykovsky reaction;
参考文献
Korotkov, Vadim S.; Larionov, Oleg V.; Hofmeister, Anja; Magull, Joerg; De Meijere, Armin
Journal of Organic Chemistry, 2007 , vol. 72, # 20 p. 7504 - 7510
反应条件
in N,N-dimethyl-formamide
T=10°C; 0.25 h;
参考文献
Izquierdo, M. L.; Arenal, I.; Bernabe, M.; Alvarez, E. Fernandez
Tetrahedron, 1985 , vol. 41, # 1 p. 215 - 220
反应条件
in methanol; diethyl ether
T=-70°C; 1 h;
参考文献
Izquierdo, M. L.; Arenal, I.; Bernabe, M.; Alvarez, E. Fernandez
Tetrahedron, 1985 , vol. 41, # 1 p. 215 - 220
反应条件
in methanol; diethyl ether
T=-70°C; 1 h;
参考文献
Izquierdo, M. L.; Arenal, I.; Bernabe, M.; Alvarez, E. Fernandez
Tetrahedron, 1985 , vol. 41, # 1 p. 215 - 220
反应条件
in water
T=25°C; different pH; Kinetics;
参考文献
Bernasconi, Claude F.; Fornarini, Simonetta
Journal of the American Chemical Society, 1980 , vol. 102, # 16 p. 5329 - 5336
反应条件
in N,N-dimethyl-formamide
Condensation; 0.5 h; Heating;
参考文献
Lipson; Orlov; Desenko; Karnozhitskaya; Shirobokova
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 5 p. 595 - 599
参考文献
Rodriguez, Hortensia; Reyes, Osvaldo; Suarez, Margarita; Garay, Hilda E.; Perez, Rolando; Cruz, Luis Javier; Verdecia, Yamila; Martin, Nazario; Seoane, Carlos
Tetrahedron Letters, 2002 , vol. 43, # 3 p. 439 - 441
反应条件
in tetrahydrofuran; diethyl ether
0.0833333 h;
参考文献
Haslego, Mark L.; Smith, Francis X.
Synthetic Communications, 1980 , vol. 10, # 6 p. 421 - 428
