反应条件
1: 95 percent / KHCO3 / dimethylformamide / 42 h / Ambient temperature
2: NaOAc, N2O4 / CCl4 / 0 °C
3: H2 / 20percent Pd(OH)2/C / 1) dioxane, 75-80 deg C, 1 h, 2) ethyl acetate, 35 psi, 20 h
View Scheme
参考文献
Karanewsky, Donald S.; Malley, Mary F.; Gougoutas, Jack Z.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3744 - 3747
