(丙烯酸氧基甲基)甲基二甲氧基硅烷合成路线 (共 3 条)
反应条件
(10H)-phenothiazine; tetra-n-butyl phosphonium chloride T=88 - 90°C; P=525.053 Torr; 3 h; Product distribution / selectivity;
参考文献
WACKER CHEMIE AG
Patent: US2012/4437 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
1: 2-methyl-2-propenoic acid With potassium hydroxide in toluene 2: (chloromethyl)dimethoxy(methyl)silane With 4,4'-bismethylene(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in toluene; butanone T=110°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1081 - 1092
反应条件
1,1-bis (3,5-di-t-butyl-4-hydroxyphenyl)-methane
参考文献
US2004/171859 A1, ;
Page 4-5 ;