5-(苯氧基甲基)-1,3,4-噻二唑-2-胺合成路线 (共 6 条)
反应条件
phosphoric acid T=120°C; 2 h;
参考文献
Sathisha; Khanum, Shaukath A.; Chandra, J.N. Narendra Sharath; Ayisha; Balaji; Marathe, Gopal K.; Gopal, Shubha; Rangappa
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 1 p. 211 - 220
反应条件
poly(ethylene glycol) supported dichlorophosphate T=120°C; 0.133333 h; microwave irradiation;
参考文献
Li, Zheng; Yu, Jin-Lan; Yang, Jing-Ya; Zhu, Wei; Zhao, Yan-Long; Xing, Yu-Lin; Wang, Xi-Cun
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 1 p. 183 - 190
反应条件
trifluoroacetic acid T=60 - 80°C; 6 h;
参考文献
Suzuki; Miwa; Aibara; Kanno; Takamori; Tsubokawa; Ryokawa; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 2 p. 357 - 363
反应条件
1: potassium carbonate / acetone / 8 h / Reflux 2: hydrazine hydrate / methanol / 1 h / 20 °C 3: ethanol / 4 h / Reflux 4: phosphoric acid / 2 h / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 1 p. 211 - 220
反应条件
1: hydrazine hydrate / methanol / 1 h / 20 °C 2: ethanol / 4 h / Reflux 3: phosphoric acid / 2 h / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 1 p. 211 - 220
反应条件
1: ethanol / 4 h / Reflux 2: phosphoric acid / 2 h / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 1 p. 211 - 220