(E)-N-甲基-1-(3-硝基苯基)甲亚胺合成路线 (共 9 条)
反应条件
sodium hydroxide in dichloromethane; water T=20 - 35°C; 2 h; Inert atmosphere;
参考文献
Connolly, Terrence J.; Constantinescu, Anton; Lane, Tim S.; Matchett, Michael; McGarry, Patrick; Paperna, Mariya
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 837 - 842
参考文献
Baldridge, Anthony; Kowalik, Janusz; Tolbert, Laren M.
Synthesis, 2010 , # 14 art. no. M06809SS, p. 2424 - 2436
反应条件
triethylamine in acetonitrile T=25°C; 48 h; Yield given;
参考文献
Cho, Bong Rae; Namgoong, Sung Keon; Bartsch, Richard A.
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1320 - 1324
反应条件
triethylamine in acetonitrile T=25°C; 48 h; Yield given;
参考文献
Cho, Bong Rae; Namgoong, Sung Keon; Kim, Tae Rin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 853 - 856
反应条件
1: N-chlorosuccinimide / pentane / 0.33 h 2: Et3N / acetonitrile / 48 h / 25 °C View Scheme
参考文献
Cho, Bong Rae; Namgoong, Sung Keon; Kim, Tae Rin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 853 - 856
反应条件
methanol; sodium methylate T=25°C; var. MeONa conc.; Rate constant;
参考文献
Cho, Bong Rae; Yoon, Jong Chan; Bartsch, Richard A.
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4943 - 4946
反应条件
water; triethylamine; zinc dibromide in chloroform-d1
参考文献
Chemistry - A European Journal, , vol. 20, # 12 p. 3288 - 3291
反应条件
water; triethylamine; zinc dibromide in chloroform-d1
参考文献
Zhang, Yan; Ramstroem, Olof
Chemistry - A European Journal, 2014 , vol. 20, # 12 p. 3288 - 3291
反应条件
sodium tetrahydroborate in methanol 1 h; Heating;
参考文献
Connolly, Terrence J.; Constantinescu, Anton; Lane, Tim S.; Matchett, Michael; McGarry, Patrick; Paperna, Mariya
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 837 - 842