N-甲基-N-(4-硝基苯基)乙酰胺合成路线 (共 15 条)
反应条件
pyridine in tetrahydrofuran T=0°C; 3 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP1813606 A1, 2007 ;
Location in patent: Page/Page column 91 ;
反应条件
nitrogen(IV) oxide; ozone in dichloromethane
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 339 - 344
反应条件
copper(l) chloride in chlorobenzene T=130°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Qinqin; Liu, Xiaolong; Zhang, Yuejiao; Chen, Chao; Chen, Wanzhi
Organic Letters, 2013 , vol. 15, # 13 p. 3326 - 3329
反应条件
potassium hydroxide; acetone
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1321
Journal of the Indian Chemical Society, , vol. 32, p. 489
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 52, p. 833,836
反应条件
2: HNO3+H2SO4 / 0 - 12 °C View Scheme
参考文献
Journal of the Chemical Society, , vol. 113, p. 690
反应条件
T=175°C; im geschlossenen Rohr;
参考文献
Chemische Berichte, , vol. 31, p. 2529
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate 1.) toluene, 30-35 deg C, 30 min, 2.) toluene, 30-35 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 21, # 18-19 p. 1889 - 1900
反应条件
lead(IV) acetate; chloroform
参考文献
Chemische Berichte, , vol. 92, p. 288,289
反应条件
1: platinum; methanol / Hydrogenation 3: aqueous HCl View Scheme
参考文献
Journal of the Chemical Society, , p. 3089,3092