4-氯-3-硝基三氟甲苯合成路线 （共 136 条）
反应条件
potassium carbonate in ethanol; water
4 h; Heating;
参考文献
King, Frank D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3381 - 3386
反应条件
1: 75 percent / K2CO3 / dimethylformamide / 1.5 h / 100 - 110 °C
2: 63 percent / Fe powder; HOAc / propan-2-ol / 1.5 h / Heating
3: pyridine / 3.5 h / -5 - 20 °C
View Scheme
参考文献
Ivanov, Vladimir V.; Yurchenko, Alexandr A.; Chernega, Alexander N.; Pinchuk, Alexandr M.; Tolmachev, Andrej A.
Heteroatom Chemistry, 2002 , vol. 13, # 1 p. 84 - 92
参考文献
Lubisch; Behl; Hofmann
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 23 p. 2887 - 2892
反应条件
in acetonitrile
T=25°C; Kinetics; Further Variations:amine concentration;
参考文献
Crampton, Michael R.; Emokpae, Thomas A.; Isanbor, Chukwuemeka
European Journal of Organic Chemistry, 2007 , # 8 p. 1378 - 1383
反应条件
sodium azide; N-ethyl-N-methylpyrrolidinium tetrafluoroborate; tetrabutylammomium bromide in water
T=60°C; 4 h;
参考文献
Sheremetev, Aleksei B.; Aleksandrova, Nataliya S.; Ignat'Ev, Nikolai V.; Schulte, Michael
Mendeleev Communications, 2012 , vol. 22, # 2 p. 95 - 97
反应条件
water; sulfur; triethylamine in tetrahydrofuran
T=80°C; P=9561.6 Torr; 10 h;
参考文献
Konishi, Ken-ichi; Nishiguchi, Ikuzo; Hirashima, Tsuneaki; Sonoda, Noboru; Murai, Shinji
Synthesis, 1984 , # 3 p. 254 - 255
