10H-吩噻嗪 5,5-二氧化物合成路线 （共 12 条）
反应条件
sodium; lithium in tetrahydrofuran 24 h; Heating;
参考文献
Farmer, Steven C.; Berg, Seth H.
Molecules, 2008 , vol. 13, # 6 p. 1345 - 1352
参考文献
Bodea; Raileanu
Acad. Repub. Pop. Rom., Fil. Cluj, Stud. Cercet. Chim., 1957 , vol. 8, p. 303,309
Chem.Abstr., 1960 , p. 0 22657
反应条件
dihydrogen peroxide; acetic acid
T=80°C; 2 h;
参考文献
Sakamoto, Kei; Kiriki, Satoshi; Ogawa, Tomonori; Shinohara, Masanobu
Patent: US2012/302675 A1, 2012 ;
Location in patent: Page/Page column 12-13 ;
参考文献
Bernstein; Rothstein
Journal of the American Chemical Society, 1944 , vol. 66, p. 1886
反应条件
immobilized tungstate(IV) thermolysin; dihydrogen peroxide in tert-butyl alcohol
T=40°C; 2 h;
参考文献
Bakker, Martin; Van Rantwijk, Fred; Sheldon, Roger A.
Canadian Journal of Chemistry, 2002 , vol. 80, # 6 p. 622 - 625
反应条件
1: 80 percent / lithium diisopropylamide / tetrahydrofuran / -78 deg C, 30 min, then allowed to warm to rt.
2: m-chloroperbenzoic acid / CH2Cl2 / 0 °C
3: methanol / 0.5 h
View Scheme
参考文献
Babudri, F.; Di Nunno, L.; Florio, S.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3883 - 3886
反应条件
1: 3.7 g / 30percent H2O2 / acetic acid / 15 h / Heating
2: aqueous NaOH
View Scheme
参考文献
Catsoulacos, P.; Pelecanou, M.; Camoutsis, Ch.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1437 - 1440
反应条件
sulfuric acid; sulfur trioxide
Erhitzen des Reaktionsprodukts mit wss. H2SO4 auf 200grad;
参考文献
I.G. Farbenind.
Patent: DE582268 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 451
参考文献
Babudri, F.; Di Nunno, L.; Florio, S.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3883 - 3886
反应条件
1: aqueous H2O2; acetic acid
2: aq.-ethanolic KOH
View Scheme
参考文献
Toei
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 1270
Chem.Abstr., 1958 , p. 961
