二氯(二环戊二烯基)铂(Ⅱ)合成路线 （共 13 条）
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Rakowsky, Margaret H.; Woolcock, John C.; Wright, Laura L.; Green, David B.; Rettig, Michael F.; Wing, Richard M.
Organometallics, 1987 , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of dicyclopentadiene was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Rakowsky, Margaret H.; Woolcock, John C.; Wright, Laura L.; Green, David B.; Rettig, Michael F.; Wing, Richard M.
Organometallics, 1987 , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Rakowsky, Margaret H.; Woolcock, John C.; Wright, Laura L.; Green, David B.; Rettig, Michael F.; Wing, Richard M.
Organometallics, 1987 , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Rakowsky, Margaret H.; Woolcock, John C.; Wright, Laura L.; Green, David B.; Rettig, Michael F.; Wing, Richard M.
Organometallics, 1987 , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Rakowsky, Margaret H.; Woolcock, John C.; Wright, Laura L.; Green, David B.; Rettig, Michael F.; Wing, Richard M.
Organometallics, 1987 , vol. 6, p. 1211 - 1218
反应条件
in dichloromethane under nitrogen, 41°C, 48 h, some decompn. obsd.; TLC monitoring, solvent removed (vac.); residue washed (warm petroleum ether; purifn. chromy. (silica, CH2Cl2/petroleum ether 2/1, v/v), crystn. from eluant solvent; mixt. of two isomers (by (19)F-NMR);
参考文献
Journal of Organometallic Chemistry, , vol. 359, p. 267 - 284
反应条件
in dichloromethane under nitrogen, 41°C, 24 h, some decompn. obsd.; TLC monitoring, solvent removed (vac.); residue washed (warm petroleum ether; chromy. (silica, CH2Cl2/petroleum ether 2/1, v/v), crystn. from eluant solvent, elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 359, p. 267 - 284
反应条件
in dichloromethane under nitrogen, 25°C, 168 h; TLC monitoring, solvent removed (vac.); residue washed (warm petroleum ether; chromy. (silica, CH2Cl2/petroleum ether 2/1, v/v), crystn. from eluant solvent, elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 359, p. 267 - 284
反应条件
in dichloromethane under nitrogen, 25°C, 264 h; TLC monitoring, solvent removed (vac.); residue washed (warm petroleum ether; chromy. (silica, CH2Cl2/petroleum ether 2/1, v/v), crystn. from eluant solvent, elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 359, p. 267 - 284
反应条件
in dichloromethane under nitrogen, 41°C, 48 h; TLC monitoring, solvent removed (vac.); residue washed (warm petroleum ether; chromy. (silica, CH2Cl2/petroleum ether 2/1, v/v), crystn. from eluant solvent, elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 359, p. 267 - 284
