hydrogenchloride in toluene byproducts: methane, Me4Si; evacuated vessel; condensation of excess HCl into soln. of V-complex, then 1 h at 20°C (pptn.);
参考文献
Razuvaev, G. A.; Bayushkin, P. Ya.; Cherkasov, V. K.; Gladyshev, E. N.; Phokeev, A. P.
Inorganica Chimica Acta, 1980 , vol. 44, p. L103 - L104
HCl in 1,4-dioxane byproducts: orotic acid; in presence of atmospheric oxygen;
参考文献
Latyaeva, V. N.; Lineva, A. N.; Zimina, S. V.; Ellert, O. G.; Arsen'eva, T. I.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 521 - 528
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 591 - 598
hydrogenchloride in not given sealed vessel, vac.;
参考文献
Razuvaev, G. A.; Latyaeva, V. N.; Gladyshev, E. N.; Krasilnikova, E. V.; Lineva, A. N.; Kozina, A. P.
Inorganica Chimica Acta, 1978 , vol. 31, p. L357 - L360
hydrogenchloride in pentane byproducts: CH4; Irradiation (UV/VIS); a soln. of Cp2VMe2 in pentane was filtered into a water-jacketed Schlenk tube under Ar, photolyzed for 48 h; pptn. (filtered, washed, dried); addn. of HCl-satd. toluene to residue; pptn.; filtration; exposing filtrate to air;; washing residue with pentane; removal of solvent from filtrate by vac.;detn. by gas chromatography, UV spectroscopy; elem. anal.;;
参考文献
Journal of Organometallic Chemistry, , vol. 287, p. 195 - 206
hydrogenchloride in pentane byproducts: CH4; Irradiation (UV/VIS); a soln. of Cp2VMe2 in pentane was filtered into a water-jacketed Schlenk tube under Ar, photolyzed for 48 h; pptn. (filtered, washed, dried); addn. of HCl-satd. toluene to residue; pptn.; filtration;; washing residue with pentane; removal of solvent from filtrate by vac.;detn. by gas chromatography, UV spectroscopy; elem. anal.;;
参考文献
Journal of Organometallic Chemistry, , vol. 287, p. 195 - 206
