反应条件
KOC(CH3)3 in tetrahydrofuran (N2); KOC(CH3)3 in THF added slowly to a soln. of Cr complex, stirred for 1 h at room temp., C10H6(OCH2OCH3)C10H5(OCH2OCH3)CHO added, refluxed for 4 h; cooled at room temp., hydrolyzed with an aq. soln. of NH4Cl, extd. (CH2Cl2), the org. layers washed (H2O), dried (MgSO4), filtered, evapd. (vac.), chromd. (silica gel, petroleum ether/EtOAc); elem. anal.;
参考文献
Organometallics, , vol. 26, # 25 p. 6139 - 6149
