(1,5-环辛二烯)二氯化铂(II)合成路线 （共 69 条）
反应条件
in ethanol byproducts: COD; 1 equiv. of NaBH4, 2 equiv. of phosphine per complex, room temp., few min, gas evolution; evapn., extn. (benzene), recrystn. (benzene/hexane);
参考文献
Inorganica Chimica Acta, , vol. 65, p. L77 - L78
反应条件
in ethanol byproducts: COD; 10 equiv. of NaBH4, 2 equiv. of phosphine per complex, room temp., few min, gas evolution; recrystn. (benzene/ethanol);
参考文献
Inorganica Chimica Acta, , vol. 65, p. L77 - L78
反应条件
in ethanol byproducts: COD; 10 equiv. of NaBH4, 2 equiv. of phosphine per complex, room temp., few min, gas evolution; recrystn. (benzene/ethanol);
参考文献
Inorganica Chimica Acta, , vol. 65, p. L77 - L78
反应条件
in tetrahydrofuran N2 or Ar-atmosphere; room temp. (12 h); filtering, washing (Et2O), drying (vac.); elem. anal.;
参考文献
Organometallics, , vol. 14, p. 4542 - 4548
反应条件
in dichloromethane 0.166667 h;
参考文献
US2005/107337 A1, ;
Page/Page column 3 ;
反应条件
triphenylphosphine in dichloromethane slow diffusion of diethyl ether in the CH2Cl2 soln., filtered off, washed with diethyl ether, dried (vac., 70°C);
参考文献
Inorganica Chimica Acta, , vol. 154, p. 89 - 94
反应条件
in dimethylsulfoxide-d6 (N2, Schlenk technique); reaction of platinum compd. and 1 equiv. of phosphine deriv. in DMSO-d6; NMR;
参考文献
Dalton Transactions, , vol. 40, # 11 p. 2588 - 2600
反应条件
in dimethylsulfoxide-d6 (N2, Schlenk technique); reaction of platinum compd. and 1 equiv. of phosphine deriv. in presence of 6 equiv. of tetrabutylammonium chloride in DMSO-d6; NMR;
参考文献
Dalton Transactions, , vol. 40, # 11 p. 2588 - 2600
反应条件
in dichloromethane 0.166667 h;
参考文献
US2005/107337 A1, ;
Page/Page column 3 ;
反应条件
triphenylphosphine in dichloromethane slow diffusion of diethyl ether in the CH2Cl2 soln., filtered off, washed with diethyl ether, dried (vac., 70°C);
参考文献
Inorganica Chimica Acta, , vol. 154, p. 89 - 94
