(1,5-环辛二烯)二氯化铂(II)合成路线 （共 69 条）
反应条件
dipotassium tetrachloroplatinate in water; acetic acid T=90°C; 0.5 h;
参考文献
EP1577300 A1, ;
Page/Page column 37 ;
反应条件
in water; acetic acid 1.16667 - 1.33333 h; Heating / reflux;
参考文献
US2005/107337 A1, ;
Page/Page column 3 ;
反应条件
HNO3; SnCl2*2H2O in further solvent(s) byproducts: nitrogen oxides; N2-atmosphere; dissoln. of Pt in aqua regia by stirring overnight at 60°C, concn., addn. of concd. HCl, evapn., dissoln. in H2O/PrOH=4:3,addn. of excess COD and slight excess SnCl2, stirring (12°C, 7 d , pptn.); filtration, washing (H2O), drying (SiO2); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 528, # 1-2 p. 163 - 178
反应条件
in water; acetic acid addn. of excess of COD (in glacial AcOH) to aq. Pt-complex soln., stirring (90°C, 1 h, pptn.); filtration, washing (EtOH, Et2O), drying (vac.);
参考文献
Inorganica Chimica Acta, , vol. 279, # 1 p. 105 - 110
反应条件
in water; acetic acid T=90°C; 1 h; Inert atmosphereSchlenk technique;
参考文献
Dalton Transactions, , vol. 43, # 6 p. 2549 - 2558
反应条件
in neat (no solvent) refluxing in excess of COD for 2 h (crystn.); collection (filtration), washing (hexane), drying (vac.); elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 289 - 292
反应条件
HCl in not given Pt-complex was treated with HCl gas;
参考文献
Organometallics, , vol. 6, p. 1766 - 1772
反应条件
acetic acid in water T=90°C;
参考文献
Dalton Transactions, , vol. 43, # 2 p. 751 - 763
反应条件
sodium hydrogencarbonate in ethanol mixt. heated (5h, 60°C); addn. of solid NaHCO3; stirring (1h); filtering; washing with divinyltetramethyldisiloxane;
参考文献
Organometallics, , vol. 10, p. 3750 - 3759
反应条件
1: hydraziniumdihydrochloride; HPtCl6·6H2O in water T=30 - 35°C; Inert atmosphere; 2: cyclooctadiene With acetic acid T=90°C; 0.5 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 20, # 11 p. 3169 - 3182
