1-苄基-4-氧代氮杂烷盐酸盐合成路线 （共 7 条）
反应条件
1: 91 percent / K2CO3 / CHCl3 / 7.5 h / Heating 2: 1) C2H5OK, 2) HCl / 1) ethanol, xylene, reflux, 16 h; 2) ethanol. View Scheme
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
1: 94 percent / K2CO3 / CHCl3 / 7 h / Heating 2: 1) C2H5OK, 2) HCl / 1) ethanol, xylene, reflux; 2) ethanol. View Scheme
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
hydrogenchloride; potassium ethanolate 1) ethanol, xylene, reflux; 2) ethanol.; Yield given. Multistep reaction;
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
hydrogenchloride; potassium ethanolate 1) ethanol, xylene, reflux, 16 h; 2) ethanol.; Yield given. Multistep reaction;
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride in toluene; benzene
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 51, # 9 p. 2034 - 2049
反应条件
water; palladium Hydrogenation;
参考文献
Yokoo; Morosawa
Bulletin of the Chemical Society of Japan, 1956 , vol. 29, p. 631
反应条件
20 palladium(II) hydroxide on carbon; hydrogen; triethylamine in ethyl acetate T=20°C; Reagent/catalyst;
参考文献
JANSSEN RandD IRELAND; GUILLEMONT, Jerôme Emile Georges; LANÇOIS, David Francis Alain; MOTTE, Magali Madeleine Simone; BALEMANS, Wendy Mia Albert; KOUL, Anil
Patent: WO2014/23815 A1, 2014 ;
Location in patent: Page/Page column 43 ;
