3-(4-叔丁基苯)-丙酸合成路线 （共 16 条）
反应条件
hydrogen; palladium 10 on activated carbon in tetrahydrofuran T=20°C; 2 h;
参考文献
AMOREPACIFIC CORPORATION
Patent: WO2006/98554 A1, 2006 ;
Location in patent: Page/Page column 43 ;
WO 2006/098554 A1
反应条件
hydrogenchloride; oxygen; 6-hydroxy-6-oxo-2,5,7,10-tetraoxa-6-phospha-tricyclo[6.3.0.04,11]undecane; copper dichloride; palladium dichloride in tetrahydrofuran; water T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Heterocycles, , vol. 63, # 12 p. 2797 - 2803
反应条件
1: With potassium carbonate; Pd-Tedicyp catalyst in N,N-dimethyl-formamide T=110°C; Heck reaction; 20 h; 2: With sodium hydroxide; water in N,N-dimethyl-formamide T=50 - 80°C;
参考文献
Lemhadri, Mhamed; Doucet, Henri; Santelli, Maurice
Tetrahedron, 2004 , vol. 60, # 50 p. 11533 - 11540
参考文献
Bulletin de la Societe Chimique de France, , p. 2615 - 2617
反应条件
1: 75 percent / triethylammonium formate 2: H2O / acetonitrile / 0.5 h / 120 °C / microwave irradiation View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 389 - 395
反应条件
oxygen in octane T=40°C; P=2250.23 Torr; KineticsMechanism; Temperature;
参考文献
Tetrahedron, , vol. 69, # 10 p. 2268 - 2275
反应条件
[Pd2Cl2(μ-Cl)2((S)-μ-3,5-xyl-phanephos)]; water; toluene-4-sulfonic acid; lithium chloride in butanone T=50°C; P=22502.3 Torr; 66 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 48 p. 9197 - 9200
反应条件
1: H2 / 10percent Pd/C / 16 h / 760 Torr / Ambient temperature 2: aq. NaOH / methanol / 2 h / Heating View Scheme
参考文献
Bioorganic Chemistry, , vol. 25, # 1 p. 63 - 75
反应条件
formic acid/triethylamine complex 5:2
参考文献
Kawasaki, Masashi; Goto, Michimasa; Kawabata, Shigeki; Kometani, Tadashi
Tetrahedron Asymmetry, 2001 , vol. 12, # 4 p. 585 - 596
反应条件
1: 2-(phenyl)ethyl bromide With iodine; magnesium in diethyl ether 2 h; Reflux; 2: 4-t-butyl vinyl benzene With (C5H3N)(MeC=N(C6H4-2,6-iPr2))2; iron(II) chloride in tetrahydrofuran T=20°C; 2 h; 3: carbon dioxide in tetrahydrofuran 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 29 p. 11900 - 11903
