4-[双-(2-氯乙基)氨基]苯甲醛合成路线 （共 47 条）
反应条件
1: With trichlorophosphate T=0 - 40°C; Vilsmeier-Haack formylation; 8 h; Inert atmosphere; 2: With potassium carbonate in water Cooling with ice;
参考文献
Massin, Julien; Dayoub, Wissam; Mulatier, Jean-Christophe; Aronica, Christophe; Bretonniere, Yann; Andraud, Chantal
Chemistry of Materials, 2011 , vol. 23, # 3 p. 862 - 873
反应条件
trichlorophosphate in N,N-dimethyl-formamide 5 h; Reflux;
参考文献
Zhang, Taiping; She, Guangwei; Qi, Xiaopeng; Mu, Lixuan
Tetrahedron, 2013 , vol. 69, # 34 p. 7102 - 7106
反应条件
trichlorophosphate T=80°C; 2 h;
参考文献
Meng, Xiang-Ming; Liu, Lei; Hu, Hui-Yuan; Zhu, Man-Zhou; Wang, Mao-Xiang; Shi, Jin; Guo, Qing-Xiang
Tetrahedron Letters, 2006 , vol. 47, # 45 p. 7961 - 7964
反应条件
trichlorophosphate in N,N-dimethyl-formamide T=90°C; 4 h; Cooling;
参考文献
Morgan, M. Thomas; Bagchi, Pritha; Fahrni, Christoph J.
Journal of the American Chemical Society, 2011 , vol. 133, # 40 p. 15906 - 15909
反应条件
trichlorophosphate; benzene
参考文献
DE711665 , ;
DRP/DRBP Org.Chem.
US2141090 , ;
Journal of the Chemical Society, , p. 489,491
反应条件
1: 69 percent / NaHCO3 / 48 h / Heating 2: 55 percent / POCl3 / 1 h / Heating 3: 70 percent / POCl3 / 2 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 55, # 7 p. 1263 - 1270
参考文献
Dhapalapur,M.G. et al.
Journal of Medicinal Chemistry, 1968 , vol. 11, # 1 p. 154 - 156
参考文献
Dhapalapur,M.G. et al.
Journal of Medicinal Chemistry, 1968 , vol. 11, # 1 p. 154 - 156
参考文献
Billman; Koehler; May
Journal of pharmaceutical sciences, 1969 , vol. 58, # 6 p. 767 - 769
参考文献
Dhapalapur,M.G. et al.
Journal of Medicinal Chemistry, 1968 , vol. 11, # 1 p. 154 - 156
