1207973-75-8合成路线 （共 13 条）
反应条件
1,1'-carbonyldiimidazole 1.) THF, room temperature, 1 h, 2.) -78 deg C, 40 min; Yield given. Multistep reaction;
参考文献
Hoffman, Robert V.; Tao, Junhua
Tetrahedron, 1997 , vol. 53, # 21 p. 7119 - 7126
反应条件
in tetrahydrofuran T=-78°C; 0.0833333 h;
参考文献
Vrielynck, Sara; Vandewalle, Maurits; Garcia, Ana M.; Mascarenas, Jose L.; Mourino, Antonio
Tetrahedron Letters, 1995 , vol. 36, # 49 p. 9023 - 9026
反应条件
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane T=-78°C; 2 h; Yield given;
参考文献
Solladie-Cavallo, Arlette; Roche, Didier; Bold, Guido; Acemoglu, Figan; Tintelnot-Blomley, Marina; Fischer, Jean; De Cian, Andre
Tetrahedron Asymmetry, 1996 , vol. 7, # 6 p. 1797 - 1810
反应条件
in tetrahydrofuran a) -78 deg C, 1 h, b) -78 to 23 deg C, 1 h; Yields of byproduct given;
参考文献
Kiselyov, Alexander S.; Strekowski, Lucjan
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4476 - 4478
反应条件
1: (i) THF, (ii) /BRN= 969135/, HMPT
2: aq. HClO4 / acetonitrile
View Scheme
参考文献
Herrmann,J.L. et al.
Tetrahedron Letters, 1973 , p. 4715 - 4718
参考文献
Kraus, George A.; Gottschalk, Peter
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2111 - 2112
反应条件
1: HMPT / tetrahydrofuran
2: NaI / acetone
3: (i) LDA, (ii) /BRN= 1862195/, THF, (iii) aq. NaOAc, AcOH
View Scheme
参考文献
Kieczykowski,G.R. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 175 - 176
参考文献
Kramer, Rainer; Brueckner, Reinhard
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6537 - 6541
参考文献
Damon,R.E. et al.
Tetrahedron Letters, 1976 , p. 2749 - 2752
参考文献
Damon,R.E. et al.
Tetrahedron Letters, 1976 , p. 2749 - 2752
