9-三氟甲基-9h-芴-9-醇合成路线 （共 11 条）
反应条件
1: C9H16N2*C3H2F6O2 With potassium tert-butylate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=-30°C; 0.5 h; 2: 9H-fluoren-9-one in N,N-dimethyl-formamide T=-30°C; 1.5 h;
参考文献
Riofski, Mark V.; Hart, Allison D.; Colby, David A.
Organic Letters, 2013 , vol. 15, # 1 p. 208 - 211
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide T=-20 - 20°C; 8.16667 h; Irradiation;
参考文献
Ait-Mohand, Samia; Takechi, Naoto; Medebielle, Maurice; Dolbier Jr., William R.
Organic Letters, 2001 , vol. 3, # 26 p. 4271 - 4273
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Jablonski, Lukas; Joubert, Jerome; Billard, Thierry; Langlois, Bernard R.
Synlett, 2003 , # 2 p. 230 - 232
反应条件
potassium tert-butylate in tetrahydrofuran T=25°C; 24 h;
参考文献
Billard, Thierry; Langlois, Bernard R.; Blond, Gaelle
European Journal of Organic Chemistry, 2001 , # 8 p. 1467 - 1471
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Jablonski, Lukas; Billard, Thierry; Langlois, Bernard R.
Tetrahedron Letters, 2003 , vol. 44, # 5 p. 1055 - 1057
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=-10°C; 12 h; zinc rod anode, nickel cathode, 0.3 A;
参考文献
Sibille, S.; Mcharek, S.; Perichon, J.
Tetrahedron, 1989 , vol. 45, # 5 p. 1423 - 1428
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Jablonski, Lukas; Joubert, Jerome; Billard, Thierry; Langlois, Bernard R.
Synlett, 2003 , # 2 p. 230 - 232
反应条件
1: With potassium tert-butylate in N,N-dimethyl-formamide T=-40 - 20°C; 1 h; 2: With hydrogenchloride in water; N,N-dimethyl-formamide T=20°C;
参考文献
Cherkupally, Prabhakar; Beier, Petr
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 252 - 255
反应条件
in benzene
1 h; Inert atmospherePhotolysis;
参考文献
Afifi, Hanan; Mikhailine, Alexandre; Mladenova, Gabriela; Chtchemelinine, Andrei; Sultana, Israt; Dyblenko, Tatiana; Danilov, Evgeny; Fournier, Rene; Lee-Ruff, Edward
Arkivoc, 2012 , vol. 2012, # 6 p. 343 - 354
反应条件
1: 1 h / |Photolysis
2: benzene / 1 h / |Photolysis
View Scheme
参考文献
Dyblenko, Tatiana; Chtchemelinine, Andrei; Reiter, Ryan; Chowdhury, Ruhul Q.; Enaya, Alexander; Afifi, Hanan; Fournier, Rene; Mladenova, Gabriela; Lever, Alfred Barry P.; Lee-Ruff, Edward
Photochemistry and Photobiology, 2014 , vol. 90, # 2 p. 470 - 475
