4-[(叔-丁基二甲基硅烷基)氧基]丁烷-2-酮合成路线 (共 12 条)
反应条件
sodium periodate in tetrahydrofuran; water T=25°C;
参考文献
Li, Jun; Menche, Dirk
Synthesis, 2009 , # 11 art. no. Z01709SS, p. 1904 - 1908
反应条件
1: triphenyl-methyl-phosphonium iodide With n-butyllithium in tetrahydrofuran
T=-78°C; 0.5 h;
2: 4-(tert-butyl-dimethyl-silyloxy)butan-2-one in tetrahydrofuran
T=-78 - 0°C; Wittig reaction; 4 h;
参考文献
Kao, Chai-Lin; Kittleman, William; Zhang, Hua; Seto, Haruo; Liu, Hung-Wen
Organic Letters, 2005 , vol. 7, # 25 p. 5677 - 5680