3,4-二甲氧基苯甲醛合成路线 (共 996 条)
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=80°C; 24 h; Inert atmosphere; Solvent;
参考文献
Gopi Krishna Reddy; Krishna; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5635 - 5640
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); N,N-dicyclohexylmethylamine; potassium formiate; tetra-(n-butyl)ammonium iodide; PCy3∙HBF4; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in acetonitrile T=80°C; 18 h; Sealed tubeGloveboxInert atmosphere;
参考文献
Korsager, Signe; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6112 - 6120
反应条件
[bis(acetoxy)iodo]benzene; oxygen in acetic acid T=80°C; P=760.051 Torr; 24 h; Solvent; chemoselective reaction;
参考文献
Zhang, Jian; Liu, Yu; Chiba, Shunsuke; Loh, Teck-Peng
Chemical Communications, 2013 , vol. 49, # 97 p. 11439 - 11441
反应条件
potassium carbonate in ethylene glycol dimethyl ether T=145°C; 0.416667 h; Microwave irradiationInert atmosphereSealed vessel;
参考文献
Maras, Nenad; Polanc, Slovenko; Kocevar, Marijan
Tetrahedron, 2008 , vol. 64, # 51 p. 11618 - 11624
反应条件
3-chloro-benzenecarboperoxoic acid; meso-tetra(2,6-dichloro-3-sulphonatophenyl)porphyrin iron chloride in methanol 2 h; Ambient temperature;
参考文献
Cui, Futong; Dolphin, David
Canadian Journal of Chemistry, 1992 , vol. 70, # 8 p. 2314 - 2318
反应条件
potassium carbonate in acetone Etherification; methylation; 0.0833333 h; microwave irradiation;
参考文献
Mitra; De; Karchaudhuri
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 5 p. 387 - 389
反应条件
3-chloro-benzenecarboperoxoic acid; meso-tetra(2,6-dichloro-3-sulphonatophenyl)porphyrin iron chloride in water 2 h; Ambient temperaturephosphate buffer, pH 3; Further byproducts given;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 8 p. 2314 - 2318
反应条件
3-chloro-benzenecarboperoxoic acid; meso-tetra(2,6-dichloro-3-sulphonatophenyl)porphyrin iron chloride in water 2 h; Ambient temperaturephosphate buffer, pH 3; Further byproducts given;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 8 p. 2314 - 2318
反应条件
4-amino-N-hydroxyphthalimide; laccase from Trametes versicolor; oxygen in water T=45°C; 22 h; pH=4.5;
参考文献
Tetrahedron Letters, , vol. 39, # 33 p. 5955 - 5956
反应条件
oxygen; cerium (IV) oxide; palladium T=120°C; P=760 Torr; 5 h;
参考文献
Tetrahedron, , vol. 62, # 28 p. 6666 - 6672