3,4-二甲氧基苯甲醛合成路线 (共 996 条)
反应条件
potassium iodide; potassium carbonate in N-methyl-acetamide; toluene
参考文献
Cheil Jedang Corp.
Patent: US6103729 A1, 2000 ;
US 6103729 A
反应条件
citric acid in ethanol
参考文献
Consortium fur elektrochemische Industrie GmbH
Patent: US6069282 A1, 2000 ;
反应条件
1: With potassium hydroxide in methanol Nef reaction; Continuous flow conditions; 2: With potassium permanganate; water in methanol T=25°C; Nef reaction; SonicationContinuous flow conditions; chemoselective reaction;
参考文献
Sedelmeier, Joerg; Ley, Steven V.; Baxendale, Ian R.; Baumann, Marcus
Organic Letters, 2010 , vol. 12, # 16 p. 3618 - 3621
反应条件
N,N,N',N,-tetramethylethylenediamine; hydrogen; palladium diacetate; propyl di-tert-butylphosphinite in toluene T=100°C; P=3750.38 Torr; 20 h; Inert atmosphere;
参考文献
Neumann, Helfried; Kadyrov, Renat; Wu, Xiao-Feng; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 10 p. 2213 - 2216
反应条件
in dichloromethane T=0°C; 48 h;
参考文献
Sun, Xiaowei; Gao, Chengzhe; Zhang, Fan; Song, Zhuang; Kong, Lingyi; Wen, Xiaoan; Sun, Hongbin
Tetrahedron, 2014 , vol. 70, # 3 p. 643 - 649
反应条件
1: With oxygen; ozone in dichloromethane T=-78°C; 2: With poly(ethylene glycol)-triphenylphosphine in dichloromethane T=-78 - 20°C;
参考文献
Sieber, Frank; Wentworth Jr., Paul; Janda, Kim D.
Molecules, 2000 , vol. 5, # 8 p. 1018 - 1032
反应条件
Bi(NO3)3; water in benzene T=20°C; 5 h;
参考文献
Komatsu, Naoki; Taniguchi, Azusa; Wada, Shinobu; Suzuki, Hitomi
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 5 p. 473 - 480
反应条件
potassium dichromate; aluminium trichloride 0.0833333 h;
参考文献
Mohammadpoor-Baltork, Iraj; Sadeghi, Majid M.; Adibi, Abol-Hassan
Molecules, 2001 , vol. 6, # 11 p. 900 - 908
参考文献
International Telephone and Telegraph Corporation
Patent: US4453017 A1, 1984 ;
反应条件
potassium carbonate; OsO4 in THF-H2O; ethyl acetate; acetone