反应条件
KOH in xylene byproducts: H2O; N2, several crystals of KOH added to the mixture of Sn-compound and theamine in xylol, stirred at 110-120°C; cooled, filtered, partial evapn. of solvent yielded tetraphenylstannane, extn. (hexane) of residue yielded spirodistannacane; elem. anal.;
参考文献
Shiryaev, V. I.; Stepina, E. M.; Tandura, S. N.; Kovaleva, E. A.; Grachev, A. A.; Androsenko, S. I.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 666 - 670
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1994 , # 4 p. 714 - 718