(1R,5S)-rel-香芹醇合成路线 (共 6 条)
反应条件
oxygen; Au-CeO2 T=119.84°C; P=750.075 Torr;
参考文献
Abad, Alberto; Corma, Avelino; Garcia, Hermenegildo
Chemistry - A European Journal, 2008 , vol. 14, # 1 p. 212 - 222
反应条件
aluminum oxide T=180°C; the reaction was carried out in the injection port of a gas chromatograph; different temperature; Product distribution;
参考文献
Kobold, Uwe; Vostrowsky, Otto; Bestmann, Hans Juergen; Kubeczka, Karl Heinz
Liebigs Annalen der Chemie, 1987 , p. 557 - 560
反应条件
aluminum oxide
T=180°C; the reaction was carried out in the injection port of a gas chromatograph; different temperature; Product distribution;
参考文献
Kobold, Uwe; Vostrowsky, Otto; Bestmann, Hans Juergen; Kubeczka, Karl Heinz
Liebigs Annalen der Chemie, 1987 , p. 557 - 560
反应条件
Multi-step reaction with 2 steps 1: NaH (50percent dispersion in oil) / N,N-dimethyl-acetamide / Ambient temperature2: chlorotrimethylsilane/conc. H2SO4 / diethyl ether / further reagents and catalysts discussed
参考文献
Sarma, J. C.; Borbaruah, M.; Sarma, D. N.; Barua, N. C.; Sharma, R. P. Tetrahedron, 1986 , vol. 42, # 14 p. 3999 - 4006
反应条件
Multi-step reaction with 3 steps 1: lithium aluminum hydride2: pyridine / 20 h / Ambient temperature3: Pseudomonas sp. NOF-5 strain / 72 h / 30 °C
参考文献
Inagaki, Takashi; Ueda, Hiroo Agricultural and Biological Chemistry, 1987 , vol. 51, # 10 p. 2635 - 2640
反应条件
Multi-step reaction with 4 steps 1: cultured cells of Nicotiana tabacum / 240 h / 25 °C2: Al(OC3H7)3 / propan-2-ol3: cultured cells of Nicotiana tabacum / 144 h / 25 °C4: H2 / Pd/C
参考文献
Hamada, Hiroki Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 869 - 878