4-[(p-甲氧基苄基)氧基]-1-丁醇合成路线 （共 9 条）
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Kumar, Pradeep; Naidu, S. Vasudeva; Gupta, Priti
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2843 - 2846
反应条件
silver(l) oxide in dichloromethane 48 h;
参考文献
Guerra, Sebastiano; Trinh, Thi Minh Nguyet; Schillinger, Franck; Muhlberger, Lucie; Sigwalt, David; Holler, Michel; Nierengarten, Jean-Francois
Tetrahedron Letters, 2013 , vol. 54, # 46 p. 6251 - 6257
反应条件
Amberlyst-15 in dichloromethane 4.5 h; Reflux; regioselective reaction;
参考文献
Chavan, Subhash P.; Harale, Kishor R.
Tetrahedron Letters, 2012 , vol. 53, # 35 p. 4683 - 4686
反应条件
ethanol; copper(ll) bromide T=20°C; 4.5 h;
参考文献
Mezaache, Rofia; Dembele, Yenimegue Albert; Bikard, Yann; Weibel, Jean-Marc; Blanc, Aurelien; Pale, Patrick
Tetrahedron Letters, 2009 , vol. 50, # 52 p. 7322 - 7326
反应条件
indium(III) chloride in water; acetonitrile 2 h; Heating;
参考文献
Yadav; Reddy, B.V. Subba; Srinivas; Maiti
Journal of Chemical Research - Part S, 2001 , # 12 p. 528 - 529
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether T=-78°C; 2 h;
参考文献
Kozikowski; Jung; Springer
Journal of the Chemical Society - Series Chemical Communications, 1988 , # 3 p. 167 - 169
反应条件
jones reagent in acetone Jones oxidation; 1.5 h;
参考文献
Hirai, Kanako; Ooi, Hidenori; Esumi, Tomoyuki; Iwabuchi, Yoshiharu; Hatakeyama, Susumi
Organic Letters, 2003 , vol. 5, # 6 p. 857 - 859
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 20°C; Swern oxidation;
参考文献
Bruenjes, Marco; Sourkouni-Argirusi, Georgia; Kirschning, Andreas
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 5 p. 635 - 642
反应条件
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C
1.2: 20 °C
2.1: toluene / 5 h / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C
View Scheme
参考文献
Pujari, Sandip A.; Gowrisankar, Parthasarathy; Kaliappan, Krishna P.
Chemistry - An Asian Journal, 2011 , vol. 6, # 11 p. 3137 - 3151
