1-氯-4-(甲氧基甲基)苯合成路线 (共 28 条)
反应条件
zinc; 5-trimethylsilyl-2,2'-bipyridine; niobium bromide in 1-methyl-pyrrolidin-2-one T=20 - 70°C; Inert atmosphere;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP2192124 A1, 2010 ;
Location in patent: Page/Page column 44 ;
反应条件
Sodium bromate; ammonia; acetic acid in water T=90°C; 4 h; Product distribution / selectivity;
参考文献
IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: EP1555257 A1, 2005 ;
Location in patent: Page/Page column 29 ;
反应条件
Sodium bromate; ammonia; water; acetic acid T=90°C; 15 h; Product distribution / selectivity;
参考文献
IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: EP1555257 A1, 2005 ;
Location in patent: Page/Page column 27 ;
反应条件
Sodium bromate; ammonia; water; acetic acid T=90°C; 15 h; Product distribution / selectivity;
参考文献
EP1555257 A1, ;
Page/Page column 27 ;
反应条件
RuO4 in water; acetone T=30°C; Rate constant;
参考文献
Acta Chemica Scandinavica, , vol. 49, # 8 p. 615 - 622
反应条件
nitric acid in dichloromethane T=20°C; 1 h;
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
参考文献
Markees
Journal of Organic Chemistry, 1958 , vol. 23, p. 1490
反应条件
potassium hydroxide in dimethyl sulfoxide
T=20°C;
参考文献
XEROX CORPORATION
Patent: US2008/255389 A1, 2008 ;
Location in patent: Page/Page column 10 ;
反应条件
1: With dicarbonyl(pentamethylcyclopentadienyl)(4-methoxyphenyl)iron in dichloromethane
4 h; Inert atmosphereIrradiationSchlenk technique;
2: With sodium hydroxide in methanol; water
Inert atmosphereSchlenk technique;
参考文献
Argouarch, Gilles; Grelaud, Guillaume; Roisnel, Thierry; Humphrey, Mark G.; Paul, Frederic
Tetrahedron Letters, 2012 , vol. 53, # 37 p. 5015 - 5018
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=80°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Ogata, Toshimi; Sano, Hiroshi; Migita, Toshihiko
Chemistry Letters, 1984 , p. 1225 - 1226