2-甲基-1-[(4-甲基苯基)磺酰基]氮丙啶合成路线 (共 8 条)
参考文献
Xu, Hao; Tian, Hua; Zheng, Liangyu; Liu, Qingwen; Wang, Li; Zhang, Suoqin
Tetrahedron Letters, 2011 , vol. 52, # 22 p. 2873 - 2875
反应条件
nonafluoro-n-butanesulfonyl fluoride; triethylamine in dichloromethane T=20°C; 1 h;
参考文献
Yan, Zhaohua; Guan, Chengbo; Yu, Zhangxin; Tian, Weisheng
Tetrahedron Letters, 2013 , vol. 54, # 43 p. 5788 - 5790
反应条件
sodium hydride in tetrahydrofuran
参考文献
Argouarch, Gilles; Gibson, Colin L; Stones, Graham; Sherrington, David C
Tetrahedron Letters, 2002 , vol. 43, # 21 p. 3795 - 3798
反应条件
1: lithium borohydride / tetrahydrofuran / 0 - 20 °C 2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 1 p. 189 - 197
反应条件
1: 90 percent / pyridine 2: 98 percent / NaH / tetrahydrofuran View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 21 p. 3795 - 3798
反应条件
1: [3H]-L-Alanine With N-ethyl-N,N-diisopropylamine 2: With lithium aluminium tetrahydride 3: p-toluenesulfonyl chloride With 4-(N,N-dimethlyamino)pyridine; triethylamine
参考文献
Pei, Yuxin; Brade, Katja; Brule, Emilie; Hagberg, Lars; Lake, Fredrik; Moberg, Christina
European Journal of Organic Chemistry, 2005 , # 13 p. 2835 - 2840
反应条件
1: LiAlH4 2: pyridine 3: KOH / methanol View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 18 p. 2517 - 2527
反应条件
Na naphthalenide in ethylene glycol dimethyl ether T=-78°C; 0.25 h; Inert atmosphere;
参考文献
Rubin, Heather; Cockrell, Jennifer; Morgan, Jeremy B.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8865 - 8871