3-氨基-2,4,5-三氟苯甲酸合成路线 （共 4 条）
反应条件
sulfuric acid; ammonium chloride; triethylamine in water T=130°C; 170 h; Sealed tube;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 129 - 136
反应条件
1: ammonia / 100 h / 110 °C / Autoclave 2: sulfuric acid; ammonium chloride; triethylamine / water / 170 h / 130 °C / Sealed tube View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 129 - 136
反应条件
hydrogenchloride; sodium nitrite in water; toluene
参考文献
Warner-Lambert Company
Patent: US4885386 A1, 1989 ;
反应条件
hydrogenchloride; tert.-butylnitrite; Copper(I)chloride in acetonitrile
参考文献
Daiichi Seiyaku Co., Ltd.
Patent: US5286723 A1, 1994 ;
