2-甲基-1,3-环己二酮合成路线 （共 134 条）
反应条件
hydrogenchloride; formaldehyd; dimethyl amine; palladium monocarbide in methanol; water
参考文献
Sumitomo Chemical Company, Limited; Sumika Fine Chemicals Co., Ltd.
Patent: US5276198 A1, 1994 ;
反应条件
sodium hydroxide; hydrogen; Rh/Al2O3 in water P=2585.7 Torr; 9.5 h; Ambient temperature;
参考文献
Liu, Hsing-Jang; Wynn, Hla
Canadian Journal of Chemistry, 1986 , vol. 64, p. 658 - 666
反应条件
in sodium hydroxide T=65°C; 24 h;
参考文献
Lertpibulpanya, Duanpen; Marsden, Stephen P.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 18 p. 3498 - 3504
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=25°C; 10.5 h;
参考文献
Journal of Organic Chemistry, , vol. 50, # 1 p. 69 - 76
反应条件
sodium dichromate; sulfuric acid in acetone
参考文献
Journal of the American Chemical Society, , vol. 108, # 8 p. 2094 - 2096
反应条件
hydrogenchloride; water in acetone T=20°C;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 20 p. 4296 - 4300
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 8 h; Heating;
参考文献
Tetrahedron, , vol. 62, # 33 p. 7809 - 7816
反应条件
1: 98 percent / PCC / CH2Cl2 / 1 h / 25 °C 2: 80 percent / aq. H2O2; NaOH / methanol / 6 h / 20 °C 3: 36 percent / Bu3SnH; AIBN / benzene / 8 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 33 p. 7809 - 7816
反应条件
1: 80 percent / aq. H2O2; NaOH / methanol / 6 h / 20 °C 2: 36 percent / Bu3SnH; AIBN / benzene / 8 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 33 p. 7809 - 7816
参考文献
Pataki; Harvey
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 20 - 22
