5-重氮基环戊并-1,3-二烯合成路线 (共 14 条)
反应条件
polymer-supported sulfonyl azide; triethylamine in acetonitrile Ambient temperature;
参考文献
Duerr, Heinz; Hauck, Gerhard; Brueck, Wolfgang; Kober, Helge
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 9 p. 1149 - 1152
反应条件
diethyl ether; lithium cyclopentadienide
参考文献
Doering; DePuy
Journal of the American Chemical Society, 1953 , vol. 75, p. 5955
反应条件
in acetonitrile T=23°C; Equilibrium constant;
参考文献
Minutolo, Filippo; Katzenellenbogen, John A.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 11 p. 1617 - 1620
反应条件
oxygen in solid matrix T=-253.2°C; Irradiationfurther with <18O>O2; Product distributionMechanism;
参考文献
Bell, Gordon A.; Dunkin, Ian R.
Journal of the Chemical Society, Chemical Communications, 1983 , # 21 p. 1213 - 1215
反应条件
oxygen T=-253.2°C; Irradiationother temperatures, different λ, reaction with (18)O(16)O and (18)O2; Mechanism;
参考文献
Dunkin, Ian R.; Shields, Charles J.
Journal of the Chemical Society, Chemical Communications, 1986 , # 2 p. 154 - 156
反应条件
T=0 - 5°C; 2.5 h; Irradiation;
参考文献
Billups; Saini, Rajesh K.; Litosh, Vladislav A.; Alemany, Lawrence B.; Wilson, William K.; Wiberg, Kenneth B.
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4436 - 4440
反应条件
in toluene T=85°C; 18 h;
参考文献
Grobe, Joseph; Van Le, Duc; Immel, Franz; Krebs, Bernt; Laege, Mechtild
Chemische Berichte, 1996 , vol. 129, # 10 p. 1271 - 1274
反应条件
T=-261.2 - -228.1°C; Irradiationin argon matrix; Product distribution;
参考文献
Nefedov, Oleg M.; Zuev, Petr S.; Maltsev, Andrey K.; Tomilov, Yuri V.
Tetrahedron Letters, 1989 , vol. 30, # 6 p. 763 - 764
反应条件
Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Kirmse, Wolfgang; Loosen, Karin; Sluma, Heinz-Dieter
Journal of the American Chemical Society, 1981 , vol. 103, # 19 p. 5935 - 5937
反应条件
Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Kirmse, Wolfgang; Loosen, Karin; Sluma, Heinz-Dieter
Journal of the American Chemical Society, 1981 , vol. 103, # 19 p. 5935 - 5937