3-乙基-2,2-二甲基环氧乙烷合成路线 (共 17 条)
反应条件
magnesium bromide in N,N-dimethyl-formamide T=130°C; 1 h;
参考文献
Petroleum Chemistry, , vol. 43, # 3 p. 167 - 169
反应条件
perchloric acid in water 5 h; Ambient temperature; Mechanism;
参考文献
Guenther, Bernd-Rainer; Kirmse, Wolfgang
Liebigs Annalen der Chemie, 1980 , # 4 p. 518 - 532
反应条件
sodium tert-pentoxide; sodium hydride; zinc(II) chloride in ethylene glycol dimethyl ether T=65°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 26, # 26 p. 3111 - 3114
反应条件
perchloric acid in water 5 h; Ambient temperature;
参考文献
Liebigs Annalen der Chemie, , # 4 p. 518 - 532
反应条件
sodium tert-pentoxide; sodium hydride; zinc(II) chloride in ethylene glycol dimethyl ether T=65°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Fort, Yves; Vanderesse, Regis; Caubere, Paul
Tetrahedron Letters, 1985 , vol. 26, # 26 p. 3111 - 3114
反应条件
in acetonitrile
T=0°C;
参考文献
Detty, Michael R.; Seidler, Mark D.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1283 - 1292
反应条件
pyridine in acetonitrile
T=20°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Detty, Michael R.; Seidler, Mark D.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1283 - 1292