119072-55-8合成路线 (共 225 条)
反应条件
titanium tetrachloride in dichloromethane T=-50 - 20°C; 3 h; other aldehyde acetals; Product distribution;
参考文献
Tetrahedron Letters, , vol. 27, # 30 p. 3505 - 3506
反应条件
T=25°C; normale Addition;
参考文献
Kharasch; McNab; Mayo
Journal of the American Chemical Society, 1933 , vol. 55, p. 2522
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du Pont de Nemours and Co.
Patent: US2058465US2058466 , 19331933 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=20°C; Reagent/catalystTemperature;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3009 - 3020
反应条件
iodine; oxygen; sodium carbonate; palladium diacetate T=100°C; P=2068.6 Torr; 3 h;
参考文献
Pri-Bar, Ilan; Schwartz, Jeffrey
Chemical Communications, 1997 , # 4 p. 347 - 348
反应条件
1: Se, DBU / tetrahydrofuran / 1 h / Heating 2: DBU, O2 / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Fujiwara, Shin-Ichi; Matsuya, Takahiro; Maeda, Hajime; Shin-Ike, Tsutomu; Kambe, Nobuaki; Sonoda, Noboru
Synlett, 1999 , # 1 p. 75 - 76
反应条件
in N-dodecane T=183°C; MechanismRate constantThermodynamic data;
参考文献
Meier, Michael; Ruechardt, Christoph
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4671 - 4674
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene 2 h; RefluxInert atmosphere;
参考文献
Boissarie, Patrick J.; Hamilton, Zoe E.; Lang, Stuart; Murphy, John A.; Suckling, Colin J.
Organic Letters, 2011 , vol. 13, # 23 p. 6256 - 6259
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene 2 h; RefluxInert atmosphere;
参考文献
Boissarie, Patrick J.; Hamilton, Zoe E.; Lang, Stuart; Murphy, John A.; Suckling, Colin J.
Organic Letters, 2011 , vol. 13, # 23 p. 6256 - 6259
反应条件
Rh(I)Cl(CO)(PMe3)2 16.5 h; Ambient temperatureIrradiation; Yield given;
参考文献
Tanaka, Masato; Sakakura, Toshiyasu; Tokunaga, Yuko; Sodeyama, Touru
Chemistry Letters, 1987 , p. 2373 - 2374
反应条件
Yield given. Multistep reaction;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298