119072-55-8合成路线 （共 225 条）
反应条件
in methanol T=20°C; 24 h;
参考文献
Shaabani, Ahmad; Soleimani, Ebrahim; Rezayan, Ali Hossein
Tetrahedron Letters, 2007 , vol. 48, # 35 p. 6137 - 6141
反应条件
Yield given. Multistep reaction;
参考文献
Guram, Anil S.; Jordan, Richard F.
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5595 - 5597
反应条件
in benzene-d6 addn. of CNt-Bu to the soln. of the iron complex, keeping at room temp. for 18 h, monitored by NMR;
参考文献
Organometallics, , vol. 13, p. 619 - 630
反应条件
in benzene-d6 addn. of CNt-Bu to a soln. of the iron complex under an atmosphere of nitrogen, react. monitored by NMR;
参考文献
Organometallics, , vol. 13, p. 619 - 630
反应条件
1: tert-butylisonitrile; 2-amino-benzenethiol in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere; 2: iodobenzene With 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 4 p. 1471 - 1477
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 4 p. 1471 - 1477
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 4 p. 1471 - 1477
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene 2 h; RefluxInert atmosphere;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
反应条件
in dichloromethane under N2 or Ar, refluxed for 3 h, solvent removed under HV; chromd. (silica gel, 0°C, CH2Cl2/Et2O (1/2)), solvent removed, pentane added; elem. anal., IR, NMR, mass spectra;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 44, # 9 p. 1023 - 1034
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
