3,7,11-三甲基月桂酸钠合成路线 （共 7 条）
反应条件
Jone's reagent in isopropyl alcohol; acetone T=0°C; 4 h; Inert atmosphere;
参考文献
Munoz, Lourdes; Guerrero, Angel
Synthesis, 2012 , vol. 44, # 6 p. 862 - 864
反应条件
1: platinum/carbon xerogel catalyst; hydrogen / ethanol / 12 h / 20 °C / Inert atmosphere 2: Jone's reagent / isopropyl alcohol; acetone / 4 h / 0 °C / Inert atmosphere View Scheme
参考文献
Munoz, Lourdes; Guerrero, Angel
Synthesis, 2012 , vol. 44, # 6 p. 862 - 864
反应条件
acetic acid; platinum Hydrogenation;
参考文献
Karrer et al.
Helvetica Chimica Acta, 1948 , vol. 31, p. 1510
反应条件
1: PBr3; petroleum ether / Erwaermen und dann Behandeln des Reaktionsprodukts mit 5prozentiger alkoh.KOH bei 80grad 2: platinum; glacial acetic acid / Hydrogenation View Scheme
参考文献
Karrer et al.
Helvetica Chimica Acta, 1948 , vol. 31, p. 1510
反应条件
palladium on activated charcoal; acetic acid Hydrogenation;
参考文献
Asano; Moroe
Yakugaku Zasshi, 1949 , vol. 69, p. 378
Chem.Abstr., 1950 , p. 3080
反应条件
1: activated. zinc; benzene / Erhitzen des Produkts auf 200grad und Verseifen des erhaltenen Isofarnesensaeureaethylesters mit 10prozentiger alkoh.KOH 2: glacial acetic acid; palladium/charcoal / Hydrogenation View Scheme
参考文献
Asano; Moroe
Yakugaku Zasshi, 1949 , vol. 69, p. 378
Chem.Abstr., 1950 , p. 3080
反应条件
1: (i) H2, Pd-CaCO3, (ii) (hydrolysis) 2: KOH / 260 °C View Scheme
参考文献
Johnstone,R.A.W.; Quan,P.M.
Journal of the Chemical Society, 1963 , p. 5706 - 5713
