2, 2'-二硫代二苯甲酸合成路线 （共 163 条）
反应条件
alkali bei der Einw. methylierender Mittel;
参考文献
Hoechster Farbw.
Patent: DE193800 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 9, p. 543
反应条件
methanol; zinc(II) chloride anschliessendes Behandeln mit Chlor und danach mit wss. NH3;
反应条件
1: thionyl chloride / Reflux 2: chlorine / tetrachloromethane / 20 °C 3: triethylamine / dichloromethane / -15 °C View Scheme
参考文献
Gopinath, Pushparathinam; Ramalingam, Krishnan; Muraleedharan, Kannoth Manheri; Karunagaran, Devarajan
MedChemComm, 2013 , vol. 4, # 4 p. 749 - 752
反应条件
1: thionyl chloride / Reflux 2: chlorine / tetrachloromethane / 20 °C 3: triethylamine / dichloromethane / -15 °C View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
diphosphorus pentasulfide; xylene
参考文献
Borgna; Vicarini; Carmellino; Pagani
Farmaco, Edizione Scientifica, 1983 , vol. 38, # 10 p. 801 - 810
参考文献
Rodionow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 536,545
Chem.Abstr., 1949 , p. 2200
反应条件
1: (i) SOCl2, dioxane, (ii) NH3 2: P2S5 / xylene / Heating View Scheme
参考文献
Wagner,G.; Richter,P.
Pharmazie, 1967 , vol. 22, p. 611 - 620
反应条件
borane-THF; boron trifluoride diethyl etherate in tetrahydrofuran T=20°C; 18 h;
参考文献
Chen; Iakovleva; Kesten; Magano; Rodriguez; Sexton; Zhang; Lee
Organic Preparations and Procedures International, 2002 , vol. 34, # 6 p. 665 - 670
反应条件
1: H2SO4 2: Ph3P / H2O; dioxane / 30 °C View Scheme
参考文献
Overman,L.E. et al.
Journal of the American Chemical Society, 1974 , vol. 96, # 19 p. 6081 - 6089
参考文献
Hutchison; Smiles
Journal of the Chemical Society, 1912 , vol. 101, p. 573
