2, 2'-二硫代二苯甲酸合成路线 （共 163 条）
反应条件
1: thionyl chloride / Reflux
2: chlorine / tetrachloromethane / 20 °C
3: triethylamine / dichloromethane / -15 °C
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1: thionyl chloride / Reflux
2: chlorine / tetrachloromethane / 20 °C
3: dichloromethane / 2 h / -15 - 20 °C
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1: 84 percent / SOCl2 / 24 h / Heating
2: 37 percent / pyridine / 8 h / 10 °C
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
(i) SOCl2, dioxane, (ii) /BRN= 605631/; Multistep reaction;
参考文献
Wagner,G.; Richter,P.
Pharmazie, 1967 , vol. 22, p. 611 - 620
反应条件
1: thionyl chloride / 24 h / |Reflux
2: bromine / dichloromethane / 12 h / |Reflux
3: triethylamine / dichloromethane / 0 - 20 °C
View Scheme
参考文献
Gopinath, Pushparathinam; Ramalingam, Krishnan; Muraleedharan, Kannoth Manheri; Karunagaran, Devarajan
MedChemComm, 2013 , vol. 4, # 4 p. 749 - 752
反应条件
1: thionyl chloride / Reflux
2: chlorine / tetrachloromethane / 20 °C
3: triethylamine / dichloromethane / -15 °C
View Scheme
参考文献
Gopinath, Pushparathinam; Ramalingam, Krishnan; Muraleedharan, Kannoth Manheri; Karunagaran, Devarajan
MedChemComm, 2013 , vol. 4, # 4 p. 749 - 752
反应条件
1: thionyl chloride / Reflux
2: dichloromethane / 0.5 h / 20 °C
View Scheme
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1: thionyl chloride / 24 h / |Reflux
2: bromine / dichloromethane / 12 h / |Reflux
3: triethylamine / dichloromethane / 0 - 20 °C
View Scheme
参考文献
Gopinath, Pushparathinam; Ramalingam, Krishnan; Muraleedharan, Kannoth Manheri; Karunagaran, Devarajan
MedChemComm, 2013 , vol. 4, # 4 p. 749 - 752
反应条件
potassium acetate
T=120°C;
参考文献
D'Silva; McClelland
Journal of the Chemical Society, 1932 , p. 2883,2886
Full Text Show Details
Bartlett; McClelland
Journal of the Chemical Society, 1934 , p. 818,820
参考文献
D'Silva; McClelland
Journal of the Chemical Society, 1932 , p. 2883,2886
