反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 - 20 °C / |Inert atmosphere
1.2: 16 h / -78 - 20 °C / |Inert atmosphere
2.1: palladium diacetate; zinc; tri-cyclo-hexyl-phosphine / toluene / 0.5 h / 90 °C / |Inert atmosphere
3.1: dihydrogen peroxide / toluene; water / 17 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Minami, Yasunori; Yamada, Kotomi; Hiyama, Tamejiro
Angewandte Chemie - International Edition, 2013 , vol. 52, # 40 p. 10611 - 10615
Angew. Chem., 2013 , vol. 125, # 40 p. 10805 - 10809
