反应条件
1: ε-caprolactone; 1,3-dimercaptopropane With diisobutylaluminium hydride in tetrahydrofuran; hexane; dichloromethane T=-78 - 20°C; 2: 1,3-dimercaptopropane With boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; 1.5 h;
参考文献
Bournaud, Chloee; Marchal, Estelle; Quintard, Adrien; Sulzer-Mosse, Sarah; Alexakis, Alexandre
Tetrahedron Asymmetry, 2010 , vol. 21, # 13-14 p. 1666 - 1673