3,4,5-三甲氧基苯甲酸合成路线 （共 210 条）
反应条件
hydrogenchloride T=108 - 112°C; 7 h;
参考文献
Tetrahedron, , vol. 37, p. 1243 - 1248
参考文献
Justus Liebigs Annalen der Chemie, , vol. 263, p. 255
反应条件
sodium in methanol 8 h; Heating;
参考文献
Tetrahedron, , vol. 37, p. 1243 - 1248
反应条件
1: 14 mg / silver oxide / dimethylformamide 2: 1.) NaOH, 2.) HCl View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 961 - 965
反应条件
1: 49 mg / 0.5 h / Heating 2: 1.) 3percent NaHCO3; 2.) KMnO4 / 1.) t-BuOH, 80 deg C, 1 h; 2.) H2O, 20 min View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 5 p. 1029 - 1036
反应条件
potassium permanganate; sodium hydrogencarbonate 1.) t-BuOH, 80 deg C, 1 h; 2.) H2O, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Phytochemistry (Elsevier), , vol. 23, # 5 p. 1029 - 1036
反应条件
oxygen; anhydrous cobalt diacetate T=110°C; P=2280 Torr; 2 h; var. catalysts; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 3 p. 1035 - 1038
反应条件
boron trichloride; potassium hydrogencarbonate; calcium carbonate 1.) CH2Cl2, -40/-60 deg C, 2 h; 2.) H2O, r.t., 30 min; 3.) H2O, acetone, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Phytochemistry (Elsevier), , vol. 23, # 5 p. 1029 - 1036
反应条件
1: tetrahydrofuran / 20 °C 2: CF3COOH / CH2Cl2 / 4 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 9 p. 1709 - 1712
反应条件
sulfuric acid; zinc 1.) methanol, reflux, 8 h, 2.) water, reflux, 10 h; Multistep reaction;
参考文献
Tetrahedron, , vol. 37, p. 1243 - 1248
