1,2-二甲基-1,1,2,2-四苯基乙硅烷合成路线 （共 27 条）
反应条件
MnI2 in tetrahydrofuran
T=-10°C; 1.33333 h;
参考文献
Fuerstner, Alois; Weidmann, Hans
Journal of Organometallic Chemistry, 1988 , vol. 354, p. 15 - 22
反应条件
1 Au/TiO2; water in ethyl acetate
T=25°C; 1 h; Overall yield = 98 percent;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
反应条件
water in 1,2-dichloro-ethane
T=65°C; 4 h; Overall yield = 76 percent; stereoselective reaction;
参考文献
Gryparis, Charis; Kidonakis, Marios; Stratakis, Manolis
Organic Letters, 2013 , vol. 15, # 23 p. 6038 - 6041
反应条件
cesium fluoride in dimethyl sulfoxide
T=20°C; 18 h; GloveboxSealed tubeInert atmosphere; Reagent/catalystSolvent;
参考文献
Lescot, Camille; Nielsen, Dennis U.; Makarov, Ilya S.; Lindhardt, Anders T.; Daasbjerg, Kim; Skrydstrup, Troels
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 6142 - 6147
反应条件
cesium fluoride in dimethyl sulfoxide
T=20°C; 18 h; GloveboxSealed tubeInert atmosphere;
参考文献
Lescot, Camille; Nielsen, Dennis U.; Makarov, Ilya S.; Lindhardt, Anders T.; Daasbjerg, Kim; Skrydstrup, Troels
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 6142 - 6147
反应条件
meta-chloroperoxybenzoic acid in benzene
T=45°C; Rate constant;
参考文献
Razuvaev, G. A.; Brevnova, T. N.; Semenov, V. V.; Kornev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 4 p. 877 - 883,773 - 778
反应条件
1 Au/TiO2 in ethyl acetate
T=25°C; 4 h; Inert atmosphere;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
