1,2-二甲基-1,1,2,2-四苯基乙硅烷合成路线 （共 27 条）
反应条件
carbon in tetrahydrofuran T=0°C; 0.0833333 h;
参考文献
Journal of Organometallic Chemistry, , vol. 354, p. 15 - 22
反应条件
(η5-C5H5)Fe(CO)2Me in N,N-dimethyl-formamide 24 h; UV-irradiation; Product distribution / selectivity;
参考文献
US2009/112013 A1, ;
Page/Page column 3 ;
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: 1-chloro-2,2-dimethylpropane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: chloromethyl phenyl thioether in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: 1-iodo-2,2-dimethylpropane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: 1-bromo-2,2-dimethylpropane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: Me3SiCH2Br in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: (iodomethyl)trimethylsilane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
in diethyl ether 3 h; Heating;
参考文献
Journal of Molecular Structure, , vol. 412, # 1-2 p. 83 - 95
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 38 p. 7052 - 7054
Angewandte Chemie, , vol. 121, # 38 p. 7186 - 7188
