反应条件
MOA; urea in nitrobenzene
byproducts: ammonia; urea, ligand, FeCl2*4H2O, ammonium molybdate were pulverized and stirred into nitrobenzene, suspn. was heated to 180-190°C for 0.5 h, maintatined for 4 h, cooled to 90°C, diluted with EtOH; filtered hot, residue was washed with boiling H2O, ppt. was boiled for 10 min each in HCl and NaOH, extd. with chlorobenzene for 3 d; elem. anal.;
参考文献
Metz, Josef; Schneider, Otto; Hanack, Michael
Inorganic Chemistry, 1984 , vol. 23, p. 1065 - 1071
