4’,5,6,7-四甲氧基黄酮合成路线 （共 34 条）
反应条件
iodine in dimethyl sulfoxide T=110°C; 4 h;
参考文献
Journal of Chemical Research, , vol. 37, # 11 p. 671 - 673
反应条件
pyridine; iodine 4 h; Heating;
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane Suzuki coupling; 18 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 12, # 22 p. 5278 - 5280
反应条件
potassium cyanide in ethanol; dichloromethane 12 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 21 p. 3759 - 3763
反应条件
1: 96 percent / AcONa / 3 h / 110 °C 2: 94 percent / BF3*Et2O / 2 h / 70 °C 3: 89 percent / KOH / ethanol / 0 - 20 °C 4: 74 percent / iodine / dimethylsulfoxide / 2 h / 190 - 200 °C View Scheme
参考文献
Molecules, , vol. 12, # 1 p. 86 - 97
反应条件
1: 89 percent / KOH / ethanol / 0 - 20 °C 2: 74 percent / iodine / dimethylsulfoxide / 2 h / 190 - 200 °C View Scheme
参考文献
Molecules, , vol. 12, # 1 p. 86 - 97
反应条件
1: 94 percent / BF3*Et2O / 2 h / 70 °C 2: 89 percent / KOH / ethanol / 0 - 20 °C 3: 74 percent / iodine / dimethylsulfoxide / 2 h / 190 - 200 °C View Scheme
参考文献
Molecules, , vol. 12, # 1 p. 86 - 97
反应条件
1: 89 percent / KOH / ethanol / 0 - 20 °C 2: 74 percent / iodine / dimethylsulfoxide / 2 h / 190 - 200 °C View Scheme
参考文献
Molecules, , vol. 12, # 1 p. 86 - 97
反应条件
1: 76 percent / dimethyl dioxirane / acetone; CH2Cl2 / 1 h / 0 - 20 °C 2: 95 percent / K2CO3 / acetone / 4 h / Heating 3: 76 percent / I2; pyridine / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 95 percent / K2CO3 / acetone / 4 h / Heating 2: 76 percent / I2; pyridine / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
