(R)-1-(3-甲氧基苯基)乙胺盐酸盐合成路线 （共 5 条）
反应条件
hydrogenchloride; water in methanol T=20°C; 12 h; Inert atmosphere;
参考文献
Rao, Ramakrishna; Shewalkar, Mukesh Padmakar; Nandipati, Ramadevi; Yadav, Jhillu Singh; Khagga, Mukkanti; Shinde, Devanand Baburao
Synthetic Communications, 2012 , vol. 42, # 4 p. 589 - 598
反应条件
1: palladium 10 on activated carbon; hydrogen / acetic acid / 48 h / 20 °C / 3102.97 Torr / Inert atmosphere 2: triethylamine / methanol / 6 h / 0 °C / Inert atmosphere 3: potassium carbonate / acetone / 0 °C / Inert atmosphere; Reflux 4: hydrogenchloride; water / methanol / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Rao, Ramakrishna; Shewalkar, Mukesh Padmakar; Nandipati, Ramadevi; Yadav, Jhillu Singh; Khagga, Mukkanti; Shinde, Devanand Baburao
Synthetic Communications, 2012 , vol. 42, # 4 p. 589 - 598
反应条件
1: titanium(IV) isopropylate / ethyl acetate / 3 h / Inert atmosphere 2: sodium tetrahydroborate / ethanol; ethyl acetate / 3 h / 0 °C / Inert atmosphere 3: palladium 10 on activated carbon; hydrogen / acetic acid / 48 h / 20 °C / 3102.97 Torr / Inert atmosphere 4: triethylamine / methanol / 6 h / 0 °C / Inert atmosphere 5: potassium carbonate / acetone / 0 °C / Inert atmosphere; Reflux 6: hydrogenchloride; water / methanol / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Rao, Ramakrishna; Shewalkar, Mukesh Padmakar; Nandipati, Ramadevi; Yadav, Jhillu Singh; Khagga, Mukkanti; Shinde, Devanand Baburao
Synthetic Communications, 2012 , vol. 42, # 4 p. 589 - 598
反应条件
1: triethylamine / methanol / 6 h / 0 °C / Inert atmosphere 2: potassium carbonate / acetone / 0 °C / Inert atmosphere; Reflux 3: hydrogenchloride; water / methanol / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Rao, Ramakrishna; Shewalkar, Mukesh Padmakar; Nandipati, Ramadevi; Yadav, Jhillu Singh; Khagga, Mukkanti; Shinde, Devanand Baburao
Synthetic Communications, 2012 , vol. 42, # 4 p. 589 - 598
反应条件
1: potassium carbonate / acetone / 0 °C / Inert atmosphere; Reflux 2: hydrogenchloride; water / methanol / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Rao, Ramakrishna; Shewalkar, Mukesh Padmakar; Nandipati, Ramadevi; Yadav, Jhillu Singh; Khagga, Mukkanti; Shinde, Devanand Baburao
Synthetic Communications, 2012 , vol. 42, # 4 p. 589 - 598
