2,2,4-三甲基-7-(2-亚甲基-1-氧代丁基)-2H-1,4-苯并恶嗪-3(4H)-酮合成路线 （共 4 条）
反应条件
acetic anhydride
T=90 - 100°C; 3 h;
参考文献
Moussavi; Depreux; Lesieur; Cotelle; Sauzieres; Plancke; Fruchart
Farmaco, 1991 , vol. 46, # 2 p. 339 - 355
反应条件
1: 80 percent / polyphosphoric acid / 1.5 h / 100 °C
2: 70 percent / aq. sodium hydroxide / Heating
3: 75 percent / sodium hydrogencarbonate / butan-2-one; H2O / 8 h / 90 °C
4: 80 percent / acetic anhydride / 3 h / 90 - 100 °C
View Scheme
参考文献
Moussavi; Depreux; Lesieur; Cotelle; Sauzieres; Plancke; Fruchart
Farmaco, 1991 , vol. 46, # 2 p. 339 - 355
反应条件
1: 75 percent / sodium hydrogencarbonate / butan-2-one; H2O / 8 h / 90 °C
2: 80 percent / acetic anhydride / 3 h / 90 - 100 °C
View Scheme
参考文献
Moussavi; Depreux; Lesieur; Cotelle; Sauzieres; Plancke; Fruchart
Farmaco, 1991 , vol. 46, # 2 p. 339 - 355
反应条件
1: 70 percent / aq. sodium hydroxide / Heating
2: 75 percent / sodium hydrogencarbonate / butan-2-one; H2O / 8 h / 90 °C
3: 80 percent / acetic anhydride / 3 h / 90 - 100 °C
View Scheme
参考文献
Moussavi; Depreux; Lesieur; Cotelle; Sauzieres; Plancke; Fruchart
Farmaco, 1991 , vol. 46, # 2 p. 339 - 355
