N-苄氧羰基-L-苯丙氨酸合成路线 （共 122 条）
反应条件
1: 1) NMM, ethyl chloroformate, 2) NMM / 1) THF, 2) DMF, r.t.
2: 25percent HBr, AcOH / Ambient temperature
3: 1) NMM, ethyl chloroformate, 2) NMM / 1) THF, 2) DMF, r.t.
View Scheme
参考文献
Hashimoto; Tamaki; Sofuku; Muramatsu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 5 p. 1533 - 1541
反应条件
1.1: SOCl2 / tetrahydrofuran / 0.33 h / 25 °C
1.2: 89 percent / tetrahydrofuran / 1 h / 25 °C
2.1: 98 percent / Et3N / acetonitrile; H2O / 20 °C
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
