3,3,5-三甲基环已醇合成路线 (共 36 条)
反应条件
isopropyl alcohol; Ni(0) nanoparticles in tetrahydrofuran T=76°C; 1 h;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
Tetrahedron, 2008 , vol. 64, # 8 p. 1847 - 1852
反应条件
NiCRASi in tetrahydrofuran T=45°C; 0.75 h;
参考文献
Fort, Y; Vanderesse, R; Caubere, P
Tetrahedron Letters, 1986 , vol. 27, # 45 p. 5487 - 5490
反应条件
zinc dihydride in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Koning, A. J. De; Boersma, J.; Kerk, G. J. M. Van Der
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 1 - 12
反应条件
(R)-DTBM-Segphos; [Cu(PPh3)2NO3]; hydrogen; sodium t-butanolate in isopropyl alcohol T=30°C; P=37503.8 Torr; 18 h; optical yield given as percent eeenantioselective reaction;
参考文献
Shimizu, Hideo; Nagano, Takuto; Sayo, Noboru; Saito, Takao; Ohshima, Takashi; Mashima, Kazushi
Synlett, 2009 , # 19 p. 3143 - 3146
反应条件
[Cu(PPh3)2NO3]; hydrogen; (2S, 4S)-(-)-2,4-bis(diphenylphosphino)pentane; sodium t-butanolate in isopropyl alcohol T=30°C; P=37503.8 Torr; 18 h; enantioselective reaction;
参考文献
Synlett, , # 19 p. 3143 - 3146
反应条件
zinc-modified cyanobrohydride in diethyl ether 6 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 50, # 11 p. 1927 - 1932
反应条件
Li(1+)*C12H28AlO3(1-) in tetrahydrofuran; hexane T=-78°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 49, # 10 p. 1717 - 1724
反应条件
carbon dioxide; hydrogen T=350°C; P=90009 Torr; Supercritical conditionsFlow reactor;
参考文献
Organic Process Research and Development, , vol. 2, # 3 p. 137 - 146
反应条件
triethylamine in acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 34, # 50 p. 8107 - 8110
Tetrahedron, , vol. 51, # 43 p. 11751 - 11764
反应条件
diethyl ether; sodium
参考文献
Justus Liebigs Annalen der Chemie, , vol. 290, p. 148