4-甲基苯磺酸-4-硝基苯酯合成路线 （共 64 条）
反应条件
1: With potassium carbonate in acetone T=20 - 25°C; 2.5 h; 2: With hydrogenchloride in water; acetone
参考文献
Dainippon Sumitomo Pharma Co., Ltd.
Patent: EP1844768 A1, 2007 ;
Location in patent: Page/Page column 34 ;
反应条件
1: bis(4-methylphenyl)-disulfide With tetrabutyl-ammonium chloride; water; chloramine-T in acetonitrile T=0°C; 0.5 h; 2: 4-nitro-phenol With triethylamine in acetonitrile T=0 - 20°C; 1 h;
参考文献
Veisi, Hojat; Ataee, Meral; Fatolahi, Leila; Lotfi, Shahram
Letters in Organic Chemistry, 2013 , vol. 10, # 2 p. 111 - 117
反应条件
1: O-(4-nitrophenyl)hydroxylamine hydrochloride With triethylamine in toluene 1 h; Inert atmosphere; 2: p-toluenesulfonyl chloride in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Bonifacio, Vasco D. B.; Kumar, Rakesh P.; Prabhakar, Sundaresan; Lobo, Ana M.
Arkivoc, 2011 , vol. 2011, # 10 p. 266 - 276
反应条件
in N,N-dimethyl-formamide
参考文献
Taylor,E.C. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2422 - 2423
反应条件
1: dihydrogen peroxide; trichlorophosphate / water; acetonitrile / 25 °C 2: Amberlite IRA-400 OH(1-)-form / water; acetonitrile / 0.33 h / 25 °C View Scheme
参考文献
Hemmati, Saba; Mojtahedi, Mohammad Majid; Abaee, Mohammad Saeed; Vafajoo, Zahra; Saremi, Shokufe Ghahri; Noroozi, Mohammad; Sedrpoushan, Alireza; Ataee, Meral
Journal of Sulfur Chemistry, 2013 , vol. 34, # 4 p. 347 - 357
反应条件
1: trichloroisocyanuric acid; tetrabutyl-ammonium chloride; water / acetonitrile / 0.5 h / 0 °C 2: triethylamine / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Hemmati, Saba; Mojtahedi, Mohammad Majid; Abaee, Mohammad Saeed; Vafajoo, Zahra; Saremi, Shokufe Ghahri; Noroozi, Mohammad; Sedrpoushan, Alireza; Ataee, Meral
Journal of Sulfur Chemistry, 2013 , vol. 34, # 4 p. 347 - 357
参考文献
Reverdin; Crepieux
Bulletin de la Societe Chimique de France, 1902 , vol. <3>27, p. 745,746
Chemische Berichte, 1902 , vol. 35, p. 1444
反应条件
1: pyridine 2: nitric acid View Scheme
参考文献
Reverdin; Crepieux
Bulletin de la Societe Chimique de France, 1902 , vol. <3>27, p. 745,746
Chemische Berichte, 1902 , vol. 35, p. 1444
参考文献
Bamberger; Rising
Chemische Berichte, 1901 , vol. 34, p. 228
反应条件
dodecyltributylphosphonium bromide T=100°C;
参考文献
Fry, Slaton R.; Pienta, Norbert J.
Journal of the American Chemical Society, 1985 , vol. 107, # 22 p. 6399 - 6400
