1-硫代-b-甲基葡萄糖甙-4-甲基苯酯合成路线 （共 26 条）
反应条件
methanol; molybdenum dichloride dioxide T=20°C; 33 h; Inert atmosphere; chemoselective reaction;
参考文献
Liu, Cheng-Yuan; Chen, Hui-Ling; Ko, Chih-Min; Chen, Chien-Tien
Tetrahedron, 2011 , vol. 67, # 5 p. 872 - 876
反应条件
1: With molybdenium(VI) dioxodichloride in dichloromethane T=20°C; 14 h; 2: With molybdenium(VI) dioxodichloride in ethanol; dichloromethane 12 h; Heating;
参考文献
Weng, Shiue-Shien; Lin, Yow-Dzer; Chen, Chien-Tien
Organic Letters, 2006 , vol. 8, # 24 p. 5633 - 5636
反应条件
1: With boron trifluoride diethyl etherate T=20°C; 8 h; 2: With methanol 16 h; Reflux;
参考文献
ACADEMIA SINICA; LIANG, Chi-ming; HUNG, Shang-cheng; CHANG, Cheng-hsiu
Patent: WO2013/184564 A1, 2013 ;
Location in patent: Paragraph 00188; 00189 ;
反应条件
1: With carbon tetrabromide in methanol 0.5 h; Irradiation; 2: in methanol T=20°C; 7.5 h;
参考文献
Chen, Ming-Yi; Patkar, Laxmikant N.; Lu, Kuo-Cheng; Lee, Adam Shih-Yuan; Lin, Chun-Cheng
Tetrahedron, 2004 , vol. 60, # 50 p. 11465 - 11475
反应条件
1: ZnCl2 / 165 °C 2: NaOMe / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 30 p. 9205 - 9213
反应条件
1: 81 percent / BF3*Et2O / CH2Cl2 / 16 h 2: 87 percent / MeONa / methanol / 1 h View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 15 p. 2195 - 2202
反应条件
1: 81 percent / BF3*Et2O / CH2Cl2 / 16 h 2: 87 percent / MeONa / methanol / 1 h View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 15 p. 2195 - 2202
反应条件
DMEG; triethylamine in water; acetonitrile T=0°C; 1 h; optical yield given as percent de;
参考文献
Chemistry Letters, , vol. 38, # 5 p. 458 - 459
反应条件
1: chloroform; ethanolic KOH-solution 2: sodium methylate; methanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 11, p. 301,305
反应条件
1: 64 percent / NaH / dimethylformamide / 1.) 30 min, 2.) 80 deg C, 3.5 h 2: acetonitrile / electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.45 V (vs standard calomel reference electrode) View Scheme
参考文献
Balovoine, Gilbert; Berteina, Sabine; Gref, Aurore; Fischer, Jean-Claude; Lubineau, Andre
Journal of Carbohydrate Chemistry, 1995 , vol. 14, # 8 p. 1217 - 1236
